A comparison of a microfocus X-ray source and a conventional sealed tube for crystal structure determination
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Modelling the experimental electron density: only the synergy of various approaches can tackle the new challengesIntroducing a Hydrogen-Bond Donor into a Weakly Nucleophilic Brønsted Base: Alkali Metal Hexamethyldisilazides (MHMDS, M=Li, Na, K, Rb and Cs) with AmmoniaHighly selective and sensitive fluorescence detection of Zn(2+) and Cd(2+) ions by using an acridine sensor.Contemporary X-ray electron-density studies using synchrotron radiation.A hybrid pixel detector at an in-house device generating stunning charge density quality data.A biomimetic domino reaction for the concise synthesis of capreomycidine and epicapreomycidine.Electron transfer between hydrogen-bonded pyridylphenols and a photoexcited rhenium(I) complex.Reaction of N-heterocyclic silylenes with thioketone: formation of silicon-sulfur three (Si-C-S)- and five (Si-C-C-C-S)-membered ring systems.Group 13 metal complexes containing the bis-(4-methylbenzoxazol-2-yl)-methanide ligand.Bis-(benzothiazol-2-yl)-amines and their metal amides: a structural comparison in the solid state.Characterization of a multicomponent lithium lithiate from a combined x-ray diffraction, NMR spectroscopy, and computational approach.A Novel Bulky Heteroaromatic-Substituted Methanide Mimicking NacNac: Bis(4,6-tert-butylbenzoxazol-2-yl)methanide in s-Block Metal Coordination.Unprecedented solvent induced inter-conversion between monomeric and dimeric silylene-zinc iodide adducts.Mixed valence η6-arene cobalt(I) and cobalt(II) compound.Triimidosulfonates as Acute Bite-Angle Chelates: Slow Relaxation of the Magnetization in Zero Field and Hysteresis Loop of a Co(II) Complex.Changing and challenging times for service crystallographyBis(4-methylbenzoxazol-2-yl)methanide in s-Block Metal CoordinationCharakterisierung eines Mehrkomponenten-Lithiumlithats durch eine Kombination von Röntgenstrukturanalyse, NMR-Spektroskopie und theoretischen StudienPolyimido Sulfur(VI) Phosphanyl Ligand in Metal ComplexationSynthesis and Characterization of a Triphenyl-Substituted Radical and an Unprecedented Formation of a Carbene-Functionalized QuinodimethaneHeterocyclic substituted methanides as promising alternatives to the ubiquitous nacnac ligandTransition metal complexes containing the S(NtBu)42− tetraimidosulfate dianionThionitrosyl- and Selenonitrosyliridium ComplexesThionitrosyl- and Selenonitrosyliridium ComplexesOn the Reactivity of the Silylene PhC(NtBu)2SiNPh2toward Organic SubstratesSymmetric and unsymmetric 3,3′-linked bispyrroles via ring-enlargement reactions of furan-derived donor–acceptor cyclopropanesSchichtstruktur von [Na(NH3)4][Indenid] mit quadratisch-planarem Na(NH3)4+-KationThe Layered Structure of [Na(NH3)4][Indenide] Containing a Square-Planar Na(NH3)4+CationFacile Access to Transition-Metal-Carbonyl Complexes with an Amidinate-Stabilized Chlorosilylene LigandSynthesis of Tetrasubstituted Alkenes through a Palladium-Catalyzed Domino Carbopalladation/CH-Activation ReactionDouble N–H bond activation of N,N′-bis-substituted hydrazines with stable N-heterocyclic silyleneA P4 Chain and Cage from Silylene-Activated White PhosphorusA P4 Chain and Cage from Silylene-Activated White PhosphorusMonoanionic N,P,S-Janus Head Tripods in s-Block Metal CoordinationEnhancing N, P, S-Janus Head Tripod Ligands by OxidationSyntheses of Iron Carbonyl N-Heterocyclic Stannylene ComplexesThree-Component Domino Knoevenagel/Hetero-Diels-Alder Reaction for the Synthesis of the Amino Sugars 2-Acetoxyforosamine and 2-Acetoxyossamine - Experimental and Theoretical ResultsNovel Multidentate Sulfur-Nitrogen Ligands with Enhanced Complexation PropertiesPure α-Metallated Benzyllithium from a Single-Crystal-to-Single-Crystal TransitionReines α-metalliertes Benzyllithium durch eine Einkristall-zu-Einkristall-Umwandlung
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P2860
A comparison of a microfocus X-ray source and a conventional sealed tube for crystal structure determination
description
article
@en
im September 2009 veröffentlichter wissenschaftlicher Artikel
@de
wetenschappelijk artikel
@nl
наукова стаття, опублікована у вересні 2009
@uk
name
A comparison of a microfocus X ...... rystal structure determination
@en
A comparison of a microfocus X ...... rystal structure determination
@nl
type
label
A comparison of a microfocus X ...... rystal structure determination
@en
A comparison of a microfocus X ...... rystal structure determination
@nl
prefLabel
A comparison of a microfocus X ...... rystal structure determination
@en
A comparison of a microfocus X ...... rystal structure determination
@nl
P2093
P1476
A comparison of a microfocus X ...... rystal structure determination
@en
P2093
Carsten Michaelsen
Daniel Stern
Dirk Leusser
Jürgen Graf
Kathrin Meindl
Michael Ruf
Thomas Schulz
P304
P356
10.1107/S0021889809030921
P577
2009-09-08T00:00:00Z